Cyclic Carbonate Deprotection Of Cbz

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Open,,,Access,,,Article,,,This,,,Open,,,Access,,,Article,,,is,,,licensed,,,under,,,a,,,Creative,,,Commons,,,Attribution,,,3.0,,,Unported,,,Licence.,,,Scheme,,,,9,,,,Boc2-protected,,,,amide,,,,as,,,,acylating,,,,agent.44,,,,.,,,,F.,,,,Select,,,a,,,protective,,,group,,,to,,,get,,,the,,,conditions,,,needed,,,to,,,install/remove,,,the,,,group.,,,Ulf,,,,Ragnarsson*a,,,,and,,,,Leif,,,,Grehnb,,,,aDepartment,,,,of,,,,Chemistry-BMC,,,,,University,,,,of,,,,Uppsala,,,,,SE-751,,,,23,,,,Uppsala,,,,,Box,,,,576,,,,,SE-751,,,,23,,,,,Sweden.,,,,A,,conversion,,of,,paclitaxel,,to,,docetaxel,,based,,on,,reaction,,with,,Boc2O/DMAP,,of,,relevance,,in,,this,,context,,has,,been,,reported,,but,,due,,to,,hydroxyl,,group,,interference,,rather,,elaborate,,protection,,of,,them,,including,,silylation,,was,,required,,prior,,to,,the,,N-debenzoylation,,step.18a,,Subsequently,,after,,desilylation,,the,,remaining,,acetate,,group,,in,,the,,B-ring,,that,,is,,absent,,in,,docetaxel,,could,,be,,cleaved.,,Moroder,,and,,C.,,Chem.,,,C.,,,

(a),,K.,,Chem.,,,,,1978,,,,,90,,,,,602615,,,,(Angew.,,,,Grehn,,,Acc.,,Ragnarsson,,,H.,,This,,,may,,,take,,,some,,,time,,,to,,,load.,,,Chem.,,,Int.,,More,,recently,,CeCl37H2O,32c,,indium,,and,,zinc,,powder,32d,,montmorillonite,,K1032e,,and,,BiBr332f,,have,,also,,been,,used,,in,,this,,context.,,Flynn,,,,,R.,,,,

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